| dc.contributor.author | Doğan, Mehmet | |
| dc.contributor.author | Gündüz, Zürriye | |
| dc.contributor.author | Kızılduman, Berna Koçer | |
| dc.contributor.author | Beyli, Pınar Turan | |
| dc.contributor.author | Turhan, Yasemin | |
| dc.contributor.author | Doğan, Serap | |
| dc.contributor.author | Diken, Mehmet Emin | |
| dc.date.accessioned | 2023-09-07T08:23:42Z | |
| dc.date.available | 2023-09-07T08:23:42Z | |
| dc.date.issued | 2022 | en_US |
| dc.identifier.issn | 1465-8011 / 1743-2898 | |
| dc.identifier.uri | https://doi.org/10.1080/14658011.2022.2106727 | |
| dc.identifier.uri | https://hdl.handle.net/20.500.12462/13331 | |
| dc.description | Ministry of Energy & Natural Resources - Turkey 2009.C0231 | en_US |
| dc.description.abstract | Nano boron oxide (B2O3) was firstly produced from granular B2O3 by ball milling under
cryogenic conditions. Then, PMMA/B2O3 nanocomposites were synthesized by melting
method and then characterized. Finally, the rheological properties of PMMA/B2O3
nanocomposite were investigated using a high pressure capillary rheometer. BraunerEmmet-Teller (BET) surface area analysis showed that the surface area of B2O3 increased
with cryogenic grinding. Transmission electron microscopy (TEM) images revealed that B2O3
particles were nano-sized. Scanning electron microscopy (SEM) images showed that the
morphology changed with the increase of B2O3 amount. The thermal stability of
nanocomposites was found to be better than PMMA. PMMA degraded in two steps, while
nanocomposites degraded in one step. It was determined that the amount of residue
increased with increasing amount of B2O3. Both PMMA and nanocomposites exhibited nonNewtonian shear thinning flow behavior. In addition, rheological data were found to be
highly compatible with the Power Law model. | en_US |
| dc.language.iso | eng | en_US |
| dc.publisher | Taylor & Francis Ltd | en_US |
| dc.relation.isversionof | 10.1080/14658011.2022.2106727 | en_US |
| dc.rights | info:eu-repo/semantics/embargoedAccess | en_US |
| dc.subject | Nanocomposite | en_US |
| dc.subject | Thermal Stability | en_US |
| dc.subject | Rheological Properties | en_US |
| dc.title | Thermal stability and rheological properties of PMMA/B2O3 nanocomposites synthesised by melting method | en_US |
| dc.type | article | en_US |
| dc.relation.journal | Plastics, Rubber and Composites | en_US |
| dc.contributor.department | Fen Edebiyat Fakültesi | en_US |
| dc.contributor.authorID | 0000-0002-3707-0497 | en_US |
| dc.identifier.volume | 52 | en_US |
| dc.identifier.issue | 3 | en_US |
| dc.identifier.startpage | 186 | en_US |
| dc.identifier.endpage | 196 | en_US |
| dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | en_US |
